One-Pot Synthesis of Nano CuO-ZnO Modified Hydrochar Derived from Chitosan and Starch for the H2S Conversion

نویسندگان

چکیده

A novel kind of hydrochar adsorbent, modified by CuO-ZnO and derived from chitosan or starch, was synthesized for H2S adsorption. The prepared adsorbent characterized BET, XRD, EDX, SEM, XPS. results showed that the contained many amino groups as functional groups, nanometer metal oxide particles had good dispersion on surface hydrochar. maximum sulfur capacity reached 28.06 mg/g-adsorbent under optimized conditions. amine group significantly reduced activation energy between conducive to rapid diffusion among lattices. Simultaneously, cationic polyacrylamide a steric stabilizer could change formation process CuO ZnO nanoparticles, which made particle size smaller, enabling them react with sufficiently easily. This both starch be promising removal.

منابع مشابه

A Modified-One Pot Synthesis of Diaminoglyoxime

The one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. By increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).

متن کامل

Nano-ZnO Catalyzed Multicomponent One-Pot Synthesis of Novel Spiro(indoline-pyranodioxine) Derivatives

A simple catalytic protocol for the synthesis of novel spiro[indoline-pyranodioxine] derivatives has been developed using ZnO nanoparticle as an efficient, green, and reusable catalyst. The derivatives are obtained in moderate to excellent yield by one-pot three-component reaction of an isatin, malononitrile/ethylcyanoacetate, and 2,2-dimethyl-1,3-dioxane-4,6-dione in absolute ethanol under con...

متن کامل

synthesis of amido alkylnaphthols using nano-magnetic particles and surfactants

we used dbsa and nano-magnetic for the synthesis of amido alkylnaphtols.

15 صفحه اول

a modified-one pot synthesis of diaminoglyoxime

the one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. by increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Catalysts

سال: 2021

ISSN: ['2073-4344']

DOI: https://doi.org/10.3390/catal11070767